Centre for Carbon Materials (CCM)
Arc Discharge Set-up
Model / Make
Custom-Made Russia
Specifications
- Electric Power (DC power) : 40-50 Kw
- Voltage : 60 Volts
- Current : 500 - 800 Amperes
- Volume of chamber : ~ 150 liters
- Max. number of graphite rods : 7 Nos.
- Vacuum of the chamber : 10-2 Pa
Details
Creates CNTs through arc-vaporization of two carbon rods placed end to end, separated by few mm, in an enclosure that is usually filled with inert gas (Helium) at low pressure. A direct current of order of few hundreds Ampere (based on Graphite Current Density), driven by a potential difference of approximately 20 - 50 V, creates a high temperature discharge between the two electrodes. The discharge vaporizes the surface of one of the carbon electrodes, and forms a small rod-shaped deposit on the other electrode. High yield of CNTs depends on the uniformity of the plasma arc, and the temperature of the deposit forming on the carbon electrode.
Centre
Centre for Carbon Materials
Fluidized Bed Reactor
Model & Make
Designed & Fabricated locally
Details
The process of fluidization occurs when a fluid (liquid or gas) is passed up through the granular material under specified conditions. When a carbon containing gas flow is introduced through the bottom of a bed of solid catalyst particles, it will move upwards through the bed via the empty spaces between the particles The solid substrate (the catalytic material upon which chemical species react) material in the fluidized bed reactor is typically supported by a porous plate. The fluid (hydrocarbon and carrier gases) is then forced through the distributor up through the solid material. Depending on the operating conditions and properties of solid phase various flow regimes carbon nano-materials can be synthesized. Used for continuous synthesis of carbon nano-materials.
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Centre for Carbon Materials
Laser Flash Apparatus
Details
Ultrasonic soldering system combines heat and ultrasonic vibration to enable the soldering on glass, ceramics, aluminium, stainless steel and other unsolderable substrates. Solder is bonded to the substrate without using any chemical agents; hence the whole soldering process is flux free. The resulting joints have a high degree of electrical conductivity, adhesive strength, air/water tightness, weather and humidity resistance.
Centre
Centre for Solar Energy Materials
Magnetron Sputtering System
Model & Make
Excel India, Mumbai
Details
Sputtering is a vacuum evaporation process which physically removes portions of a coating material called the target, and deposits thin, firmly bonded onto an adjacent surface called the substrate.
The process occurs by bombarding the surface of the sputtering target with gaseous ions under high voltage acceleration. As these ions collide with the target, atoms or occasionally entire molecules of the target material are ejected and propelled against the substrate, where they form a very tight bond. The resulting coating is held firmly to the surface by mechanical forces, although, in some cases, and alloy or chemical bond may result. Since the coating material is passed into the vapor phase by a mechanical rather than a chemical or thermal process, virtually any material can be deposited. Direct current is used to sputter conductive materials.
DC magnetron sputtering system can deposit catalyst particles like Iron, Nickel, Cobalt etc on substrate materials for the growth of carbon nanotubes.
Centre
Centre for Carbon Materials
Rheometer: R/S-CPS+ Brookfield USA
B. Model & Make
R/S-CPS+, Brookfield, USA
Specification
- Torque Range : 0.05 to 50 m Nm
- Speed Range : 0.01 to 1,000 rpm
- Temperature Range : -20 to 250oC
- Shear rate Range : 0 to 6000 per sec
- Shear stress Rate : 0 to 16000 Pa
- Viscosity Range : 0.05 to 10,000 Pa s
- Spindle type : Cone and Plate type
Details
It allows the Rheological characterization (viscosity measurements) of both Newtonian and Non-Newtonian fluids; A broad measurement range, testing for yield properties and the ability to flow properties of fluids with delicate structures. This Rheometer is a rotational controlled stress instrument with geometries (cone and Plate). The geometry is directly connected to the motor shaft. A current is applied to the Rheometer motor, and the resulting speed (RPM) is measured with an optical encoder directly connected to the motor shaft. The applied Torque is converted to shear stress, and the RPM is converted to shear rate by the instrument electronics. It will be operated on controlled shear stress or controlled shear rate mode where a feed back loop is used.
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Centre for Carbon Materials
Simultaneous Thermal Analyzer (STA)
A) Model & Make
STA 449 Jupiter - Netzsch GmbH, Germany
Specifications
- TG-DTA-DSC over the range Rt-1550oC
- Heating rate : 0.01 to 999oC and isothermal between 0 and 99 h 59 min
- Vacuum : 4 m bar
- Sample mounting : Vertical
- Temp Resolution : ±0.1oC
- Temp accuracy : ±0.5oC
- Data evaluation rate: 0.120/m to 1200/m (for heating rates 0.01oC/m- 50oC/m)
- Sample volume : 0.3ml/0.085ml (DTA/DSC)
- Cp: Cp calibration, Calculation and graphic representation, temperature dependent and curve comparison
Details
Measures TGA/DTA and DSC simultaneously from room temperature to 1400 C.
In STA, the sample is subjected to a controlled temperature programme of heating where the change in mass, the absolute sample temperature and the difference in temperature of sample with a reference are measured simultaneously and monitored very accurately. With a proper calibration the heat flux to and from the sample can be calculated which in turn helps in determining the specific heat as a function of temperature. The specific heat of a material is an important thermodynamic parameter which helps to study and understand the mechanism of phase transitions etc.
Centre
Centre for Carbon Materials
Source meter
A) Model & Make
2461 Keithley & Tektronix
Details
It is a high precision instrument for high-current source meter and source measurement unit (SMU) with advanced Touch and Test facilities. It has graphical user interface (GUI) which enables the scientist/student to analyze and understand faster and work smarter.
Features
- Precision power supply with V and I read back
- True current source
- Digital multimeter (DCV, DC), ohms, and power with 6 1/2 -digit resolution
- Precision electronic load
- Pulse generator
- Trigger controller
- Voltage capability - Minimum (+ -) 100 nV and Maximum (+ -) 100 V
- Current capability - Minimum (+ -) 1 pA and Maximum (+ -) 10 A
- Max Pulse Current – 10 A
- DC/Pulse Power – 100W/1000W
- Digitizers – Dual 18-bit 1MS/s
- Wideband Noise - <4.5 mVrms type
- Sweep Types – Linear, Log, Dual Linear, Dual Log, Custom
- Reading Buffer Size - >2 Million Point
- Programming Command Type – SCPI Programming + TSP Scripting
- PC Interface – GPIB, USB, Ethernet (LXI)
- Signal Input Connections –Front: Banana Jacks, Rear: Mass Screw Terminal Connection
Applications
Solar cells and Panels, LEDs testing, Electrochemical cells and batteries testing, Sensors I-V testing and so on
Centre
Centre for Carbon Materials
Thermo Mechanical Analysis (TMA)
Details
Measures sample dimensional changes under conditions of controlled temperature, time, force, and atmosphere.
Offers all the major deformation modes necessary to characterize a wide range of materials such as solids, foams, films, and fibers. These include expansion, penetration, compression, tension, and 3-point bending.
Measures material deformation changes under controlled conditions of force, atmosphere, time and temperature. Force can be applied in compression, flexural, or tensile modes of deformation using specially designed probes.
Measures intrinsic material properties (e.g., expansion coefficient, glass transition, Young's modulus), plus processing/ product performance parameters (e.g., softening points).
Centre
Centre for Carbon Materials
workstation Biologic
A) Model & Make
BCS-805, Bio-Logic Science Instruments
Specifications
- Number of Channels: 08 Nos.
- Current range: 5: 100mA down to 10μA
- Voltage Range: 0 V ~ 10 V
- Acquisition time: 2ms
- EIS range : 10 kHz to 10mHz
- Power consumption: 60 W
Details
Bio Logic Instruments BCS-805 is a multi-channel testing system designed for R& D and production of batteries and other electrochemical energy storage devices. Each channel operates independently of each other enabling users to run tests on multiple batteries at the same time.
Applications: Battery & Intercalation Compounds, Battery Cycling, Capacitor and supercapacitor, EIS
Centre
Centre for Carbon Materials
Zetasizer
Model & Make
Nano ZS90 (green laser), Malvern Ltd UK
Specifications
- Size range for Particle size analysis: 1nm to 3 nm (diameter)
- size range for Zeta potential: 5nm to 10 nm (diameter)
Details
- Properties that can be measured by Zetasizer are (1) Particle Size and (2) Zeta potential measurements.
- Particle size analysis- The Zetasizer system determines the size by first measuring the Brownian motion of the particles in a sample using Dynamic Light Scattering (DLS) and relates this to the size of the particle. Brownian motion is the movement of particles due to the random collision with the molecules of the liquid that surrounds the particle. An important feature of Brownian motion for DLS is that small particles move quickly and large particles move more slowly. The relation between the size of the particle and its speed due to Brownian motion is defined in the Stokes-Einstein equation.
- Zeta potential measurements- Zetasizer calculates the zeta potential by determining the electrophoretic mobility and then applying the Henry equation. The electrophoretic mobility is obtained by performing an electrophoresis experiment on the sample and measuring the velocity of the particles using Laser Doppler Velocimetry (LDV).